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    Optical properties, biaxial flexural strength, and reliability of new-generation lithium disilicate glass-ceramics after thermal cycling
    (Wiley, 2022) Turksayar, Almira Ada Diken; Demirel, Munir; Donmez, Mustafa Borga
    PurposeTo investigate the color stability, translucency, biaxial flexural strength (BFS), and reliability of nano-lithium disilicate and fully crystallized lithium disilicate after thermal cycling and to compare with those of a commonly used lithium disilicate. Materials and methodsThree lithium disilicate glass-ceramics were used to prepare disk-shaped specimens (o:12 mm, thickness: 1.2 mm) from A2 shaded HT blocks (Amber Mill, AM; Initial LiSi Block, IN; IPS e.max CAD, EX). AM and EX specimens were crystallized, and all specimens were polished with a polishing paste (Diamond Polish Mint). A spectrophotometer (CM-26d) was used to measure color coordinates before and after thermal cycling. BFS test was performed after thermal cycling. Color differences (Delta E-00) and relative translucency parameter (RTP) values were calculated. One-way analysis of variance (ANOVA) (Delta E-00 and BFS), two-way ANOVA followed by Tukey's HSD tests (RTP), and chi-square tests (Weibull modulus and characteristic strength) were used for the statistical analyses (alpha = 0.05). ResultsNo significant differences were observed among the Delta E-00 values of tested materials (df = 2, F = 2.933, p = 0.070). RTP values were only affected by material type (p < 0.001) as AM had the highest RTP (p < 0.001), whereas IN and EX had similar values (p >= 0.165). BFS values varied among tested materials (df = 2, F = 21.341, p < 0.001). AM and EX had similar BFS values (p = 0.067) that were higher than that of IN (p <= 0.001). Weibull moduli of the materials were similar (p = 0.305), whereas EX had the highest and IN had the lowest characteristic strength values (p < 0.001) ConclusionsAlthough nano-lithium disilicate had the highest translucency, all materials had imperceptible color and translucency changes after thermal cycling when reported threshold values were considered. Newly introduced lithium disilicate glass-ceramics had adequate flexural strength as compared to the precursor material.
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    Trueness and precision of mandibular complete-arch implant scans when different data acquisition methods are used
    (Elsevier Sci Ltd, 2023) Demirel, Munir; Donmez, Mustafa Borga; Sahmali, Sevil Meral
    Objectives: To evaluate the effect of different data acquisition methods on the trueness and precision of mandibular complete-arch implant scans.Methods: An edentulous polyurethane master mandibular model with 6 implants was digitized by using an industrial-grade blue light scanner (ATOS Core 80 5MP) to obtain a master standard tessellation language (MSTL) file. The master model was also digitized by using either direct digital workflow with a stereoscopic camera (iCam 4D (IM)) or intraoral scanners (CEREC Primescan (PS) and Trios 4 (T4)) or indirect digital workflow with laboratory scanners (inEos X5 (X5) and CARES 7 (S7)) to obtain test-scan STLs (n = 10). All STL files were imported into a metrology-grade analysis software (Geomagic Control X 2020.1) and test-scan STLs were superimposed over MSTL. The root mean square method was used to calculate surface deviations, while angular deviations were also calculated. Kruskal-Wallis and Dunn's tests were used to evaluate measured deviations (surface and angular) for trueness and precision (alpha = 0.05).Results: X5 and S7 had the lowest, and IM had the highest surface deviations (P <= .036). The angular deviations of PS were lower than those of X5, S7, and IM (P <= .008). When surface deviations were considered, T4 had the lowest precision among tested scanners (P <= .002), and the scans of IM had higher precision than those of PS (P = .003). Scanner type did not affect the precision of the scans when angular deviations were considered (P = .084).Conclusions: The data acquisition method affected the trueness (surface and angular deviations) and precision (surface deviations) of mandibular complete-arch implant scans. Clinical significance: Tested data acquisition methods may be feasible to digitize mandibular complete-arch implants considering the deviations of the scans, which were in the range of previously reported thresholds, and the high precision of scans. However, the frameworks fabricated with the direct digital workflow that involves the scans of the stereoscopic camera might require more adjustments than those fabricated by using the scans of other tested scanners.