A new analytical protocol for the determination of cadmium in sunflower oil samples: Micro–sampling cold vapor generation–atomic absorption spectrometry after spraying based microextraction method

Basit Öğe Kaydı
dc.authorscopusidSüleyman Bodur / 57202493954
dc.authorwosidSüleyman Bodur / AHB-4581-2022
dc.contributor.authorBodur, Süleyman
dc.contributor.authorTutar, Bahar Karademir
dc.contributor.authorBodur, Sezin Erarpat
dc.contributor.authorTutar, Ömer Faruk
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2025-06-10T11:16:03Z
dc.date.available2025-06-10T11:16:03Z
dc.date.issued2025
dc.departmentİstinye Üniversitesi, Eczacılık Fakültesi, Eczacılık Temel Bilimleri Bölümü
dc.description.abstractThis study presents a new analytical method for the determination of cadmium at trace levels in sunflower oil using vortex assisted reverse phase-spraying–based fine droplet formation liquid phase microextraction method (VA-RP-SFDF-LPME), followed by micro–sampling cold vapor generation–atomic absorption spectrometry (CVG-AAS) system. Micro-sampling – gas liquid separator unit was custom designed in our laboratory to transfer the analyte–rich phase to the CVG-AAS system. Under the optimum conditions of the VA-RP-SFDF-LPME-micro–sampling-CVG-AAS method, the limit of detection, limit of quantitation and working dynamic range were found as 0.13 μg/kg, 0.44 μg/kg and 0.53–10.39 μg/kg, respectively. The percent recovery results for the spiked sunflower samples ranged from 87.6 % to 101.1 %. The greenness and practicality of developed method were assessed using AGREEprep and BAGI tools, which scored 0.27 and 62.5 points, respectively. This method offers an effective and environmentally friendly solution for detecting cadmium contamination in edible oil samples. © 2025 Elsevier Ltd
dc.identifier.citationBodur, S., Tutar, B. K., Bodur, S. E., Tutar, Ö. F., & Bakırdere, S. (2025). A new analytical protocol for the determination of cadmium in sunflower oil samples: Micro–sampling cold vapor generation–atomic absorption spectrometry after spraying based microextraction method. Food Chemistry, 144738.
dc.identifier.doi10.1016/j.foodchem.2025.144738
dc.identifier.issn03088146
dc.identifier.pmid40382906
dc.identifier.scopusqualityQ1
dc.identifier.urihttp://dx.doi.org/10.1016/j.foodchem.2025.144738
dc.identifier.urihttps://hdl.handle.net/20.500.12713/7299
dc.identifier.volume487
dc.identifier.wosWOS:001496552600006
dc.identifier.wosqualityQ1
dc.indekslendigikaynakScopus
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakPubMed
dc.institutionauthorBodur, Süleyman
dc.institutionauthoridSüleyman Bodur / 0000-0002-2994-9047
dc.language.isoen
dc.publisherElsevier Ltd
dc.relation.ispartofFood Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectAtomic Absorption Spectrometry
dc.subjectCadmium
dc.subjectMicro–Sampling Cold Vapor Generation
dc.subjectSpraying Based Microextraction
dc.titleA new analytical protocol for the determination of cadmium in sunflower oil samples: Micro–sampling cold vapor generation–atomic absorption spectrometry after spraying based microextraction method
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
1-s2.0-S0308814625019892-main.pdf
Boyut:
2.18 MB
Biçim:
Adobe Portable Document Format
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
license.txt
Boyut:
1.17 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Eczacılık Temel Bilimleri Bölümü Makale Koleksiyonu