A powerful combination of liquid chromatography-triple quadrupole mass spectrometry and quadruple isotope dilution strategy for the determination of fenuron at trace levels in river water, stream water and fruit juice samples

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dc.authoridBodur, Süleyman/0000-0002-2994-9047
dc.authoridBAKIRDERE, Sezgin/0000-0001-9746-3682
dc.authoridERARPAT BODUR, Sezin/0000-0002-9879-6662
dc.authorwosidBodur, Süleyman/AHB-4581-2022
dc.authorwosidBAKIRDERE, Sezgin/ABU-6359-2022
dc.authorwosidERARPAT BODUR, Sezin/AAZ-6733-2020
dc.contributor.authorBodur, Sueleyman
dc.contributor.authorErarpat, Sezin
dc.contributor.authorGunkara, Omer Tahir
dc.contributor.authorBakirdere, Sezgin
dc.date.accessioned2024-05-19T14:41:31Z
dc.date.available2024-05-19T14:41:31Z
dc.date.issued2023
dc.departmentİstinye Üniversitesien_US
dc.description.abstractAn accurate, sensitive, and rapid analysis methodology for the determination of fenuron at ultratrace levels in river water, stream water and fruit juice samples was developed based on quadruple isotope dilution (ID4) and liquid chromatography-triple quadrupole mass spectrometry (LC-MS/MS) system. Fenuron-d6 as isotopically labelled material (ILM) was synthesized in our laboratory to apply the ID4 method. Optimization studies were performed to find experimental conditions for the separation and detection of fenuron at trace levels. Analytical performance parameters such as limit of detection (LOD), limit of quantitation (LOQ) and linear range were determined by external calibration strategy. LOD and LOQ values for the analyte were found at ppt levels and a wide linear range was obtained in the range of 0.11 - 492.4 & mu;g/kg. Recovery studies were also carried out for water and fruit juice samples to test applicability and accuracy of the developed LC-MS/MS system. ID4 strategy was applied to the selected samples to increase accuracy of the developed method and tolerate high matrix effects for fruit juice samples. According to high percent recoveries and low relative standard deviation values, the developed LC-ID4-MS/MS system was proven as an accurate, precise and sensitive analytical method for the quantification of fenuron at trace levels.en_US
dc.identifier.doi10.1016/j.jfca.2023.105563
dc.identifier.issn0889-1575
dc.identifier.issn1096-0481
dc.identifier.scopus2-s2.0-85165921946en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://doi.org10.1016/j.jfca.2023.105563
dc.identifier.urihttps://hdl.handle.net/20.500.12713/5120
dc.identifier.volume123en_US
dc.identifier.wosWOS:001047670100001en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherAcademic Press Inc Elsevier Scienceen_US
dc.relation.ispartofJournal of Food Composition and Analysisen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz20240519_kaen_US
dc.subjectFenuronen_US
dc.subjectQuadruple Isotope Dilutionen_US
dc.subjectLiquid Chromatography-Triple Quadrupole Massen_US
dc.subjectSpectrometryen_US
dc.titleA powerful combination of liquid chromatography-triple quadrupole mass spectrometry and quadruple isotope dilution strategy for the determination of fenuron at trace levels in river water, stream water and fruit juice samplesen_US
dc.typeArticleen_US

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