Cadmium determination at trace levels in lake water samples by cold vapor generation-atomic absorption spectrometry after magnetic dispersive solid phase extraction

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dc.authoridERARPAT BODUR, Sezin/0000-0002-9879-6662
dc.authoridBAKIRDERE, Sezgin/0000-0001-9746-3682
dc.authoridBodur, Süleyman/0000-0002-2994-9047
dc.authoridKayin, Inci/0000-0003-1602-1140
dc.authorwosidERARPAT BODUR, Sezin/AAZ-6733-2020
dc.authorwosidBAKIRDERE, Sezgin/ABU-6359-2022
dc.authorwosidBodur, Süleyman/AHB-4581-2022
dc.contributor.authorBodur, Suleyman
dc.contributor.authorErarpat, Sezin
dc.contributor.authorKayin, Inci
dc.contributor.authorBakirdere, Sezgin
dc.date.accessioned2024-05-19T14:39:45Z
dc.date.available2024-05-19T14:39:45Z
dc.date.issued2023
dc.departmentİstinye Üniversitesien_US
dc.description.abstractThis study established an analytical method based on manganese ferrite based magnetic dispersive solid phase extraction (MDSPE) before cold vapor generation-atomic absorption spectrometry (CVG-AAS) for the determination of cadmium at trace levels in lake water samples collected from Horseshoe Island, Antarctica. Manganese ferrite nanoparticles were synthesized to be used as an adsorbent in the MDSPE method. Different MDSPE and CVG parameters were fixed to their optimum values after univariate optimization approach. Under the optimum conditions, analytical performance of the developed MDSPE-CVG-AAS method was evaluated and its applicability/accuracy was determined by recovery experiments. Twelve different lake water samples collected from Horseshoe Island, Antarctica were analyzed. Matrix matching calibration strategy was used to eliminate possible matrix effects arising from the lake water samples. Good recovery results (93.2-112.5%) were obtained from the spiked samples that indicated the method suitability to real samples.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [119Z846]en_US
dc.description.sponsorshipThis work with a grant number of 119Z846 was supported by The Scientific and Technological Research Council of Turkey (TUBITAK).en_US
dc.identifier.doi10.1007/s11696-023-02963-5
dc.identifier.endpage6636en_US
dc.identifier.issn0366-6352
dc.identifier.issn2585-7290
dc.identifier.issue11en_US
dc.identifier.scopus2-s2.0-85164796215en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage6629en_US
dc.identifier.urihttps://doi.org10.1007/s11696-023-02963-5
dc.identifier.urihttps://hdl.handle.net/20.500.12713/4841
dc.identifier.volume77en_US
dc.identifier.wosWOS:001028410700001en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringer Int Publ Agen_US
dc.relation.ispartofChemical Papersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmz20240519_kaen_US
dc.subjectCadmiumen_US
dc.subjectAntarcticaen_US
dc.subjectManganese Ferrite Nanoparticleen_US
dc.subjectCold Vapor Generationen_US
dc.subjectMagnetic Dispersive Solid Phase Extractionen_US
dc.titleCadmium determination at trace levels in lake water samples by cold vapor generation-atomic absorption spectrometry after magnetic dispersive solid phase extractionen_US
dc.typeArticleen_US

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