A simple spray assisted extraction/preconcentration of cadmium from sunflower oil, olive oil and hazelnut oil samples prior to flame atomic absorption spectrometry determination
Yükleniyor...
Tarih
2023
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Academic Press Inc.
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
In this study, an efficient and simple analytical approach for the preconcentration and extraction of cadmium from sunflower oil, olive oil and hazelnut oil samples using environmentally friendly, easy and efficient vortex assisted reverse phase spray-based fine droplet formation liquid phase microextraction (VA-RP-SFDF-LPME) prior to flame atomic absorption spectrometry (FAAS) measurement was proposed. Limit of detection (LOD)/limit of quantification (LOQ) values were calculated as 2.89/9.62 µg/kg, 2.00/6.68 µg/kg and 4.77/15.92 µg/kg for sunflower oil, olive oil and hazelnut oil, respectively. Recovery experiments were carried out for the evaluation of applicability and accuracy of the developed method. Satisfactory recovery results for hazelnut oil, olive oil and sunflower oil samples were recorded in the range of 92.8 – 111.9%, 96.6 – 108.2% and 90.0 – 105.7%, respectively. These results verified that the proposed method can be accurately applied to the hazelnut oil, olive oil and sunflower oil samples to qualify/quantify their cadmium content. © 2023 Elsevier Inc.
Açıklama
Anahtar Kelimeler
Cadmium, Hazelnut Oil, Microextraction, Olive Oil, Sunflower Oil
Kaynak
Journal of Food Composition and Analysis
WoS Q Değeri
N/A
Scopus Q Değeri
Q1
Cilt
117
Sayı
Künye
Bodur, S., Erarpat, S., Tutar, Ö. F., & Bakırdere, S. (2023). A simple spray assisted extraction/preconcentration of cadmium from sunflower oil, olive oil and hazelnut oil samples prior to flame atomic absorption spectrometry determination. Journal of Food Composition and Analysis, 105144.
