Trace determination of nickel in water samples by slotted quartz tube-flame atomic absorption spectrometry after dispersive assisted simultaneous complexation and extraction strategy

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dc.authoridMehmet Yusuf Kocabaş / 0000-0002-7934-6500
dc.authorscopusidMehmet Yusuf Kocabaş / 36161020700
dc.authorwosidMehmet Yusuf Kocabaş / T-2964-2017
dc.contributor.authorÖzzeybek, Gözde
dc.contributor.authorAlacakoç, Bihter
dc.contributor.authorKocabaş, Mehmet Yusuf
dc.contributor.authorBakirdere, Emine Gülhan
dc.contributor.authorChormey, Dotse Selali
dc.contributor.authorBakirdere, Sezgin
dc.date.accessioned2020-08-30T20:07:21Z
dc.date.available2020-08-30T20:07:21Z
dc.date.issued2018
dc.departmentİstinye Üniversitesi, Hastaneen_US
dc.description.abstractThis study presents a new method for the determination of nickel in aqueous samples by slotted quartz tube-flame atomic absorption spectrometry (SQT-FAAS) after a dispersive assisted simultaneous complexation and extraction (DASCE) process. Synthesized ligand was directly dissolved in the extraction solvent to eliminate the complex formation step prior to the extraction. All parameters of the SQT-FAAS and DASCE method were systematically optimized to improve the detection power of nickel for trace determinations. Under the optimum experimental conditions, the optimized method (DASCE-SQT-FAAS) recorded 137-fold enhancement in detection power over the conventional FAAS. The limits of detection and quantification were determined to be 1.6 mu g/L and 5.2 mu g/L, respectively. The calibration plot was linear over a wide concentration range and the precision for replicate measurements was appreciably high. Nickel was not detected in five different water samples but spiked recovery tests for three samples yielded results that were close to 100%, confirming the method's accuracy and applicability to the matrices tested.en_US
dc.identifier.citationOzzeybek, G., Alacakoc, B., Kocabas, M. Y., Bakirdere, E. G., Chormey, D. S., & Bakirdere, S. (2018). Trace determination of nickel in water samples by slotted quartz tube-flame atomic absorption spectrometry after dispersive assisted simultaneous complexation and extraction strategy. ENVIRONMENTAL MONITORING AND ASSESSMENT, 190(9). https://doi.org/10.1007/s10661-018-6884-zen_US
dc.identifier.doi10.1007/s10661-018-6884-zen_US
dc.identifier.issn0167-6369en_US
dc.identifier.issn1573-2959en_US
dc.identifier.issue9en_US
dc.identifier.pmid30073415en_US
dc.identifier.scopus2-s2.0-85051186923en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.urihttps://doi.org/10.1007/s10661-018-6884-z
dc.identifier.urihttps://hdl.handle.net/20.500.12713/748
dc.identifier.volume190en_US
dc.identifier.wosWOS:000440748000002en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorKocabaş, Mehmet Yusufen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofEnvironmental Monitoring and Assessmenten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectNickelen_US
dc.subjectPreconcentrationen_US
dc.subjectDasceen_US
dc.subjectSqten_US
dc.subjectFaasen_US
dc.titleTrace determination of nickel in water samples by slotted quartz tube-flame atomic absorption spectrometry after dispersive assisted simultaneous complexation and extraction strategyen_US
dc.typeArticleen_US

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